I'm only using the DCC to push the FSB a bit.
Put generally, the easiest way of OCing a Intel mobo and CPU goes like this (I'm assuming you haven't tried this plus I'm talking in general, not specifically for the 975xbx):
CPU works with multiplier, normally locked except on XE cpu's. Because it's locked, we must then use FSB OCing to raise performance. BUT, seeing that the FSB has a relation to the memory (1:1 / 2:3 / 3:2), one must keep this in mind when increasing the FSB, as the Memory will increase along with this (ie 1:1 means 1mhz up on FSB = 1mhz up on Memory).
With a 800FSB, we have CPU at 200mhz x 4, and this 200mhz will run on the memory (200x2 double data rate) aswell assuming 1:1. But, if you have 800FSB (200), with DDR2 533, then memory is running above the CPU bus at 266.5mhz - 3:2.
Now, if you have 800FSB, and DDR2 533, the easiest would be to set DDR in BIOS to 400mhz. Then, when you increase the FSB to 860 (215x4), the memory will increase at 1:1, and become 430mhz (215x2). This allows you to boost the FSB while still running under the memory's maximum (for DDR2 533 this might be 540mhz max).
You can almost safely push the FSB to 266 (whatever the the multiplier might be - ie 266x16= 4256mhz), and then only will the memory go to it's design speed. Memory timings also play a critical role, so make sure that they are stock standard once locked under their performance - you CAN set tighter timings if the memory is running below it's speed, but you are gradually OC'ing the FSB, so leave it as is for starters.
Please note, this is an example - so don't throw this right away at your setup!!! Use increments of 1-5mhz on the FSB with the DDR locked below it's design speed, test for awhile and look at the temps. If you get to the point where you are running high frequency and Windows dont wanna boot, post again cause then you probably at the limit with default voltages - someone can tell you more than I can about increasing the voltage on CPU in order to get XP to boot if OC'ing.